Thioacetamide → 4-(Benzyloxy)-3-cyanobenzenecarbothioamide
반응식
Cl.O1CCOCC1.[CH2:8]([O:15][C:16]1[CH:23]=[CH:22][C:19]([C:20]#[N:21])=[CH:18][C:17]=1[C:24]#[N:25])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C(N)(=[S:28])C>CN(C=O)C>[CH2:8]([O:15][C:16]1[CH:23]=[CH:22][C:19]([C:20](=[S:28])[NH2:21])=[CH:18][C:17]=1[C:24]#[N:25])[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1참가 물질
5
반응 조건
- 온도
- 60 °C
실험 절차
A 4M HCl/1,4-dioxane solution was added to a DMF solution of 4-(benzyloxy)isophthalonitrile and thioacetamide, followed by stirring at 60° C. to obtain 4-(benzyloxy)-3-cyanobenzenecarbothioamide. AP: 291 (Na).
출처 및 근거
- ORD 기록
- ord-cbbaf9ce9e0443d8a67a01c83ef22338
- 출처 데이터셋
- uspto-grants-2011_11
- 특허 번호
- US08067446B2
반응 노트
불러오는 중…