Ethanol → Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate

HRID 563531

반응식

HRID 563531 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH2:9][C:10]([OH:12])=[O:11])[CH:5]=[CH:6][C:7]=1[OH:8].S(=O)(=O)(O)O.[CH3:18][CH2:19]O>>[CH2:18]([O:11][C:10](=[O:12])[CH2:9][C:4]1[CH:5]=[CH:6][C:7]([OH:8])=[C:2]([Br:1])[CH:3]=1)[CH3:19]

참가 물질

4

반응물 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 27696283-Bromo-4-hydroxyphenylacetic acid

생성물 1

HCID 18620106Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate

실험 절차

(3-Bromo-4-hydroxy-phenyl)-acetic acid (5.6 mmol) in EtOH (20 mL) was treated with sulfuric acid (1 mL) and stirred at room temperature over the weekend. The mixture was concentrated to give the title compound.

후처리

  1. concentrationThe mixture was concentrated

출처 및 근거

ORD 기록
ord-434516121a0b4996ae885f5f0b5347c6
출처 데이터셋
uspto-grants-2011_11
특허 번호
US08067445B2

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