Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
반응 단계
A solution of 3-bromo-4-methoxyphenylacetic acid (3.0 g, 12.2 mmol) in EtOH and sulfuric acid was stirred at 100° C. for 2 hours. The mixture was concentrated and partitioned between EtOAc and H2O, and the organic layer was separated to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08067445B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-e3d6e9063a61482c9b1a0e69f21c57b7 |
| 출처 메모 | uspto-grants-2011_11 |