Benzyl isocyanate → HCID 44389623, 화합물
반응식
[SH:1][CH2:2][C:3]([NH:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][NH:11]C(NC1C=CC=CC=1)=O)=[O:4].[CH2:21]([N:28]=[C:29]=[O:30])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[CH2:21]([NH:28][C:29](=[O:30])[NH:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][NH:5][C:3](=[O:4])[CH2:2][SH:1])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1참가 물질
3
실험 절차
Compound 11 was prepared using the methodology described for the preparation of Compound 9, by substituting phenylisocyanate with benzylisocyanate. 1H NMR (300 MHz, DMSO-d6) δ (ppm) 7.98 (br s, 1H), 7.35-7.18 (m, 5H), 6.27 (br s, 1H), 5.91 (br s, 1H), 4.19 (s, 2H), 3.07 (d, J=8.1 Hz, 2H), 3.02 (m, 4H), 2.71 (t, J=8.1 Hz, 1H), 1.37 (m, 4H), 1.26 (m, 2H). 13C NMR (75 MHz, DMSO-d6) δ (ppm) 169.4, 158.1, 141.0, 128.2, 127.0, 126.5, 42.9, 39.2, 38.8, 29.7, 28.7, 27.1, 23.7.
출처 및 근거
- ORD 기록
- ord-e48e72a27dc84667ab452e3d18921fb9
- 출처 데이터셋
- uspto-grants-2011_11