Guanidine Hydrochloride → HCID 178479357, 화합물
반응식
O[N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[C:3]1[C:11]([O:13]C)=O.[ClH:15].[NH2:16][C:17]([NH2:19])=[NH:18].C[O-:21].[Na+]>CO>[ClH:15].[OH:21][NH:18][C:17]([NH2:19])=[N:16][C:11]([C:3]1[NH:2][C:10]2[C:5]([CH:4]=1)=[CH:6][CH:7]=[CH:8][CH:9]=2)=[O:13]참가 물질
5
실험 절차
The reaction was carried out in a manner similar to Example 1 except for using 1.00 g (5.23 mmol) of methyl 1-hydroxy-2-indolecarboxylate, 5.00 g (52.3 mmol) of guanidine hydrochloride and 50 ml of a methanol solution of 2.82 g (52.3 mmol) of sodium methoxide. 1-Hydroxy-2-indoloylguanidine hydrochloride was obtained in an amount of 0.56 g (42.0%).
출처 및 근거
- ORD 기록
- ord-5d945b79aca149fe946f2468721b1def
- 출처 데이터셋
- uspto-grants-2001_01
- 특허 번호
- US06169107A
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