1-Bromohexane → HCID 11732181, 화합물

HRID 565073노트

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HRID 565073 반응식
[Cl:1][C:2]1[CH:14]=[CH:13][C:12]2[C:11]3[C:6](=[CH:7][C:8]([Cl:15])=[CH:9][CH:10]=3)[CH2:5][C:4]=2[CH:3]=1.Br[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[Cl:1][C:2]1[CH:14]=[CH:13][C:12]2[C:11]3[C:6](=[CH:7][C:8]([Cl:15])=[CH:9][CH:10]=3)[C:5]([CH2:13][CH2:14][CH2:2][CH2:3][CH2:4][CH3:12])([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[C:4]=2[CH:3]=1

참가 물질

3

반응물 2

HCID 81011-BromohexaneHCID 2519872,7-Dichlorofluorene

생성물 1

HCID 11732181HCID 11732181, 화합물수율 91%

실험 절차

2,7-Dichloro-9,9-di(1-hexyl)fluorene is prepared from 2,7-dichlorofluorene and 1-bromohexane following the procedure of Example 1 as colorless crystals (recrystallized from hexane) in 91 percent yield, melting point 66° C to 67° C. HPLC analysis shows that the sample is 99 percent or greater pure and the spectral data confirms the title structure.

후처리

  1. customas colorless crystals (recrystallized from hexane) in 91 percent yield, melting point 66° C to 67° C

출처 및 근거

ORD 기록
ord-698411adb43748fe926436278c27f780
출처 데이터셋
uspto-grants-2001_01
특허 번호
US06169163A

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