Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phthalic Anhydride → 2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phthalic Anhydride | HCID 6811 | — |
| 반응물 | 3-(Diethylamino)phenol | HCID 7062 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acid | HCID 79878 | — |
반응 단계
2-(2′-Carboxybenzoyl)-5-diethylaminophenol was prepared as follows. A mixture of m-diethylaminophenol (1 mole) and phthalic anhydride (1.2 moles) was refluxed in toluene (2.0 L) for about 16 hours, cooled, and the resulting solid filtered, washed with toluene and dried to give 2-(2′-carboxybenzoyl)-5-diethylaminophenol in 70% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06169185A |
| 출처 데이터셋 | uspto-grants-2001_01 |
| ORD ID | ord-6101d14e85e44ff5aac0ecc59b3cd271 |
| 출처 메모 | uspto-grants-2001_01 |