3-Nonanone → HCID 72599204, 화합물

HRID 566319

반응식

HRID 566319 반응식
[CH3:1][CH2:2][C:3](=O)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])(=[O:14])[NH:12][NH2:13]>C1CCCCC1>[CH2:2]([C:3](=[N:13][NH:12][C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])=[O:14])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:1]

참가 물질

4

반응물 2

HCID 612353-NonanoneHCID 70091tert-Butyl carbazate

생성물 1

HCID 72599204HCID 72599204, 화합물

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

16.42 g (115 mmol) of 3-nonanone and 15.26 g (115.4 mmol) of tert-butyl carbazate are refluxed for 3 hours in 200 ml of cyclohexane. The solvent is removed in vacuo. This gives 30.54 g (product contains water) of a white solid, Rf=0.49 (cyclohexane/ethyl acetate=3:1).

후처리

  1. customThe solvent is removed in vacuo

출처 및 근거

ORD 기록
ord-44ffbfeb61be4a119fd1fc00e4af78ea
출처 데이터셋
uspto-grants-2001_01
특허 번호
US06174884B1

연결된 노트

불러오는 중…