Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Decanone → tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Decanone | HCID 12203 | — |
| 반응물 | tert-Butyl carbazate | HCID 70091 | — |
| 용매 | Cyclohexane heptane | HCID 21477393 | — |
| 생성물 | tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate | HCID 72599202 | 93% |
반응 단계
24.76 g (158 mmol) of 4-decanone and 20.94 g (158 mmol) of tert-butyl carbazate are heated for 90 minutes at 80° C. in 250 ml of cyclohexane/heptane mixture (1:1). After cooling, 39.71 g (93%) of a white solid are obtained by crystallization.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06174884B1 |
| 출처 데이터셋 | uspto-grants-2001_01 |
| ORD ID | ord-37087aa4fed64276a09e56a8bf9701c7 |
| 출처 메모 | uspto-grants-2001_01 |