참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tetrahydrophthalic anhydride | HCID 6810 | — |
| 반응물 | Octadecylamine | HCID 15793 | — |
| 생성물 | HCID 21266144 | HCID 21266144 | 98.7% |
반응 단계
Octadecylamine (5.31 g) was added to 4,7,3a,7a-tetrahydroisobenzofuran-1,3-dione (3.00 g). After being stirred for 2 hours at 110° C., the reaction mixture was purified by silica gel column chromatography (silica gel 80 g, chloroform), thereby yielding the entitled compound (7.85 g) as yellow crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06174885B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_01 |
|---|
| ORD ID | ord-ad23ef1d4f0946fd99ee776370455660 |
|---|
| 출처 메모 | uspto-grants-2001_01 |
|---|
