Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyloxyamine hydrochloride → 2-Benzyloxy-5-bromo-benzo[de]isoquinoline-1,3-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyloxyamine hydrochloride | HCID 102312 | — |
| 반응물 | 5-Bromobenzo[de]isochromene-1,3-dione | HCID 3907491 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-Benzyloxy-5-bromo-benzo[de]isoquinoline-1,3-dione | HCID 22623899 | 89.1% |
반응 단계
O-Benzyl hydroxylamine hydrochloride (0.9 g, 5.6 mmol) and 3-bromo-1,8-naphthalic anhydride (1.3 g, 4.7 mmol, from Example N) were reacted in pyridine (30 mL) following the procedure of Example D to give 1.6 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06177423B1 |
| 출처 데이터셋 | uspto-grants-2001_01 |
| ORD ID | ord-03ec6581c64c40e6a9e19c9659ee0cf9 |
| 출처 메모 | uspto-grants-2001_01 |