Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridinium hydrochloride → 4-Chloro-2-(5-methoxy-2-oxo-1,2-dihydropyridin-4-yl)benzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridinium hydrochloride | HCID 21584435 | — |
| 반응물 | 4-Chloro-2-(2,5-dimethoxypyridin-4-yl)benzonitrile | HCID 117605216 | — |
| 생성물 | 4-Chloro-2-(5-methoxy-2-oxo-1,2-dihydropyridin-4-yl)benzonitrile | HCID 117604935 | — |
반응 단계
7.23 g (purity 92%, 24.21 mmol) of 4-chloro-2-(2,5-dimethoxypyridin-4-yl)benzonitrile and pyridinium hydrochloride were reacted according to General Method 3A. Yield: 6.66 g (purity 91%, 96% of theory)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434690B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-98ee7d7df32b4f6189a8ec6c730c6824 |
| 출처 메모 | uspto-grants-2016_09 |