Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Difluorobenzoyl chloride → 2-(2,6-Difluoro-phenyl)-5-methyl-benzo[d][1,3]oxazin-4-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Difluorobenzoyl chloride | HCID 87438 | — |
| 반응물 | 6-Methylanthranilic acid | HCID 151210 | — |
| 반응물 | 6-Acetamido-(2,6-difluoro-phenyl)-benzo[d][1,3]oxazin-4-one | HCID 9948813 | — |
| 용매 | Toluene triethylamine | HCID 22504574 | — |
| 생성물 | 2-(2,6-Difluoro-phenyl)-5-methyl-benzo[d][1,3]oxazin-4-one | HCID 21262479 | — |
반응 단계
2-Amino-6-methylbenzoic acid (0.498 g), 2,6-difluorobenzoyl chloride (0.93 mL) and triethyl amine/toluene (1/1) (20 mL) were reacted as described under (10).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06180625B2 |
| 출처 데이터셋 | uspto-grants-2001_01 |
| ORD ID | ord-3b042ae8eaad4006bc28228c70a460e6 |
| 출처 메모 | uspto-grants-2001_01 |