O-Phenylenediamine → N-(2-Aminophenyl)-3-methylbenzenesulfonamide

HRID 568020노트

반응식

HRID 568020 반응식
[C:1]1([CH3:11])[CH:6]=[CH:5][CH:4]=[C:3]([S:7](Cl)(=[O:9])=[O:8])[CH:2]=1.[C:12]1([NH2:19])[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[NH2:18]>>[C:1]1([CH3:11])[CH:6]=[CH:5][CH:4]=[C:3]([S:7]([NH:18][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=2[NH2:19])(=[O:9])=[O:8])[CH:2]=1

참가 물질

3

반응물 2

HCID 7243O-PhenylenediamineHCID 27345953-Methylbenzenesulphonyl chloride

생성물 1

HCID 16773320N-(2-Aminophenyl)-3-methylbenzenesulfonamide

실험 절차

The sulfonamide was synthesized from 3-tolylsulfonyl chloride(0.01 mol) and o-phenylene diamine(0.01 mol) by general Method C. It was purified by recrystallization from EtOH(0.73g, 28%). EI-MS m/z 263 (M+H)+.

후처리

  1. customIt was purified by recrystallization from EtOH(0.73g, 28%)

출처 및 근거

ORD 기록
ord-fb97612670f04d55ad3bc8c875985fe4
출처 데이터셋
uspto-grants-2001_01
특허 번호
US06180675B2

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