참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Pyridinium chloride | HCID 10176127 | — |
| 반응물 | 2,3-Dichloro-4-methoxy-4'-fluorobenzophenone | HCID 20150631 | — |
| 생성물 | 2,3-Dichloro-4-hydroxy-4'-fluorobenzophenone | HCID 13015707 | — |
반응 단계
A mixture of 39.5 g of 2,3-dichloro-4-methoxy-4'-fluorobenzophenone and 160 g of pyridine hydrochloride is heated at 200° C. for one hour. The reaction mixture is poured into ice water with stirring and a precipitate forms. The precipitate is filtered and dried for about 18 hours to yield 2,3-dichloro-4-hydroxy-4'-fluorobenzophenone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04728662 |
|---|
| 출처 데이터셋 | uspto-grants-1988_03 |
|---|
| ORD ID | ord-141736b1040f4f7890ebde6cb00d9c9d |
|---|
| 출처 메모 | uspto-grants-1988_03 |
|---|
