Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → N,N-diethyl-4-iodobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | 4-Iodobenzoyl chloride | HCID 74373 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | N,N-diethyl-4-iodobenzamide | HCID 875218 | 89.7% |
반응 단계
4-Iodobenzoyl chloride (10.0 g) was added portionwise to diethylamine (2.92 g) in triethylamine (40 ml) at 20°. The resulting slurry was stirred at room temperature for 1 h, diluted with ER (150 ml), filtered and evaporated to give the title compound as an orange solid (10.2 g) m.p. 68°-70°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04730008 |
| 출처 데이터셋 | uspto-grants-1988_03 |
| ORD ID | ord-887f5a3b3710439bad711194767794ab |
| 출처 메모 | uspto-grants-1988_03 |