Nitroethane → HCID 54489179, 화합물

HRID 569090노트

반응식

C(OC(C1N=CC2NC3C(C=2C=1C)=C(C=O)C=CC=3)=O)C.[N+](CC)([O-])=O.[CH2:27]([O:29][C:30]([C:32]1[N:33]=[CH:34][C:35]2[NH:36][C:37]3[C:42]([C:43]=2[C:44]=1[CH3:45])=[C:41]([CH:46]=[C:47]([N+:49]([O-])=O)[CH3:48])[CH:40]=[CH:39][CH:38]=3)=[O:31])[CH3:28]>>[CH2:27]([O:29][C:30]([C:32]1[N:33]=[CH:34][C:35]2[NH:36][C:37]3[C:42]([C:43]=2[C:44]=1[CH3:45])=[C:41]([CH2:46][CH:47]([NH2:49])[CH3:48])[CH:40]=[CH:39][CH:38]=3)=[O:31])[CH3:28]

참가 물질

반응물 3

HCID 6587Nitroethane

HCID 54371401HCID 54371401, 화합물

HCID 54456541HCID 54456541, 화합물

생성물 1

HCID 54489179HCID 54489179, 화합물

실험 절차

The production takes places analogously to example 9 by condensation of 5-formyl-4-methyl-beta-carboline-3-carboxylic acid ethyl ester with nitroethane and hydrogenation of the resulting 4-methyl-5-(2-nitropropenyl)-beta-carboline-3-carboxylic acid ethyl ester.

출처 및 근거

ORD 기록: ord-53dcf68ea3eb4d2d9a1b095195bc16aa
출처 데이터셋: uspto-grants-1988_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04731365

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