Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfamide → HCID 178479209, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfamide | HCID 82267 | — |
| 반응물 | 3-Chloropropionitrile hydrogen chloride | HCID 86742043 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 178479209 | HCID 178479209 | — |
반응 단계
To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04731479 |
| 출처 데이터셋 | uspto-grants-1988_03 |
| ORD ID | ord-3edc6a87650c40d881e2ef0137c4c5f3 |
| 출처 메모 | uspto-grants-1988_03 |