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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 569455생성일: 2026년 10월 25일

Potassium Carbonate → 2-(Oxiran-2-yl)benzene-1-sulfonamide

https://huagongshe.com/reaction/569455

반응식

참여 물질

역할이름HCID투입량
반응물Potassium CarbonateHCID 11430—
반응물2-EthenylbenzenesulfonamideHCID 11367403—
용매ChloroformHCID 6212—
생성물2-(Oxiran-2-yl)benzene-1-sulfonamideHCID 13884523—

반응 단계

A solution consisting of 2-ethenylbenzenesulfonamide (1.5 g, 8.1 mmol) m-chloroperbenzoic acid (1.4 g, 8.1 mmol) and potassium carbonate (1.1 g, 8.1 mmol) in 150 ml of chloroform was stirred for 4 days at room temperature. The reaction was filtered and the filtrate was washed with saturated sodium bicarbonate. The organic layer was separated, dried and concentrated. The resulting oil was flash chromatographed (methylene chloride) to yield the subject compound as a white solid, m.p. 136°-139° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04732604
출처 데이터셋uspto-grants-1988_03
ORD IDord-61218c3e69fa460da834ee153f38e71b
출처 메모uspto-grants-1988_03