Methanol → 5-(2,1-Benzisothiazol-6-yl)-2,4-imidazolidinedione
반응식
[N:1]1[S:2][CH:3]=[C:4]2[CH:9]=[CH:8][C:7]([CH:10]=O)=[CH:6][C:5]=12.[CH3:12][OH:13].[C-]#N.[Na+].[C:17](=[O:20])([O-])[O-].[NH4+:21].[NH4+:22]>C(O)C.O>[N:1]1[S:2][CH:3]=[C:4]2[CH:9]=[CH:8][C:7]([CH:10]3[NH:22][C:12](=[O:13])[NH:21][C:17]3=[O:20])=[CH:6][C:5]=12참가 물질
7
실험 절차
18.6 g (0.114 mole) of 10c are stirred analogously to Example 1c in ethanol, methanol and water with 8.4 g (0.171 mole) of sodium cyanide and 43.8 g (0.456 mole) of ammonium carbonate at 60° C. for 16 hours.
출처 및 근거
- ORD 기록
- ord-23669f41ba574c43847900f1d46071d8
- 출처 데이터셋
- uspto-grants-1988_03
- 특허 번호
- US04734407
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