Methanethiol → HCID 14698107, 화합물
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[CH3:1][SH:2].F[C:4]1[CH:18]=[CH:17][C:7]([C:8]([C:10]2[S:14][C:13](=[O:15])[NH:12][C:11]=2[CH3:16])=[O:9])=[CH:6][CH:5]=1>C(O)C>[CH3:16][C:11]1[NH:12][C:13](=[O:15])[S:14][C:10]=1[C:8](=[O:9])[C:7]1[CH:17]=[CH:18][C:4]([S:2][CH3:1])=[CH:5][CH:6]=1참가 물질
4
실험 절차
Gaseus methylmercaptan is added to a solution of 5-(4-fluorobenzoyl)-4-methyl-2(3H)-thiazolone (4.7 g) in ethanol (200 ml) to saturation. The mixture is heated at 120° C. in a sealed stainless steel container for 16 hours. After cooling to ambient temperature, the mixture is evaporated to dryness. The residue is recrystallized twice from ethanol to give the title compound.
후처리
- customthe mixture is evaporated to dryness
- customThe residue is recrystallized twice from ethanol
출처 및 근거
- ORD 기록
- ord-fbab24ef11c248bdad4a086061127c68
- 출처 데이터셋
- uspto-grants-1988_03
- 특허 번호
- US04734422
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