Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 1-Trityl-4-methoxymethylpyrazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | (1-Trityl-1H-pyrazol-4-yl)methanol | HCID 10688521 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Trityl-4-methoxymethylpyrazole | HCID 68530902 | 93% |
반응 단계
This compound is obtained by reacting 1-trityl-4-hydroxymethylpyrazole (555 mg; 1.63 mmol) in dry tetrahydrofuran with sodium hydride (98 mg; 2.44 mmol) and iodomethane (0.5 mL; 8.15 mmol). Yield: 93% (536 mg, 1.51 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09023315B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-43ed1bcb2315415481cb713c6d8ab10b |
| 출처 메모 | uspto-grants-2015_05 |