Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 3-Hydroxy-N,N,2-trimethylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | 3-Hydroxy-2-methylbenzoic Acid | HCID 252023 | — |
| 생성물 | 3-Hydroxy-N,N,2-trimethylbenzamide | HCID 57753838 | 42% |
반응 단계
The title compound was prepared from 3-hydroxy-2-methylbenzoic acid and dimethylamine, using the same method as that described for preparation 75, as a solid in 42% yield. 1H NMR (400 MHz, CDCl3) δ: 1.95 (s, 3H), 2.70 (s, 3H), 2.95 (s, 3H), 6.55 (d, 1H), 6.80 (d, 1H), 7.00 (m, 1H), 9.50 (s, 1H); LRMS APCI m/z 180 [M+H]+
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09023872B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-21988550690c4b0f8bb5cefb1ccba954 |
| 출처 메모 | uspto-grants-2015_05 |