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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 571588생성일: 2026년 10월 27일

9-Phenylanthracene → 9-Bromo-10-phenyl-anthracene

https://huagongshe.com/reaction/571588

반응식

참여 물질

역할이름HCID투입량
반응물9-PhenylanthraceneHCID 11766—
반응물BromosuccinimideHCID 38309—
용매DimethylformamideHCID 6228—
생성물9-Bromo-10-phenyl-anthraceneHCID 415583689.3%

반응 단계

An amount of 13.65 (53.7 mmol) of 9-phenylanthracene was dissolved in 100 ml of N,N dimethylformamide. An amount of 10.5 g (59 mmol) of N bromosuccinimide was added and allowed to react for six hours. Then, distilled water was added to stop the reaction and the deposit was filtered. The recovered deposit was purified by column chromatography to obtain 15.97 g (48 mmol) of 9-bromo-10-phenylanthracene. The yield was 89.3%.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09028976B2
출처 데이터셋uspto-grants-2015_05
ORD IDord-56710cff061b48a6b28fa13d1d514b10
출처 메모uspto-grants-2015_05