Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9-Phenylanthracene → 9-Bromo-10-phenyl-anthracene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9-Phenylanthracene | HCID 11766 | — |
| 반응물 | Bromosuccinimide | HCID 38309 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 9-Bromo-10-phenyl-anthracene | HCID 4155836 | 89.3% |
반응 단계
An amount of 13.65 (53.7 mmol) of 9-phenylanthracene was dissolved in 100 ml of N,N dimethylformamide. An amount of 10.5 g (59 mmol) of N bromosuccinimide was added and allowed to react for six hours. Then, distilled water was added to stop the reaction and the deposit was filtered. The recovered deposit was purified by column chromatography to obtain 15.97 g (48 mmol) of 9-bromo-10-phenylanthracene. The yield was 89.3%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09028976B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-56710cff061b48a6b28fa13d1d514b10 |
| 출처 메모 | uspto-grants-2015_05 |