P-Toluenesulfonamide → 5-(tetradecyloxy)-N-tosylfuran-2-carboxamide

반응식

[CH2:1]([O:15][C:16]1[O:20][C:19]([C:21]([OH:23])=O)=[CH:18][CH:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[CH3:24][C:25]1[CH:30]=[CH:29][C:28]([S:31]([NH2:34])(=[O:33])=[O:32])=[CH:27][CH:26]=1>>[CH2:1]([O:15][C:16]1[O:20][C:19]([C:21]([NH:34][S:31]([C:28]2[CH:29]=[CH:30][C:25]([CH3:24])=[CH:26][CH:27]=2)(=[O:32])=[O:33])=[O:23])=[CH:18][CH:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

참가 물질

반응물 2

HCID 6269P-Toluenesulfonamide

HCID 1151755-(Tetradecyloxy)-2-furoic acid

생성물 1

HCID 498697595-(tetradecyloxy)-N-tosylfuran-2-carboxamide

실험 절차

The title compound was prepared as described in Example 1 starting from 0.228 g (0.7 mmol) of 5-(tetradecyloxy)furan-2-carboxylic acid and 0.361 g (2.1 mmol) of 4-methylbenzenesulfonamide. MS (m/z, ES−): 476.63 (M+1, 100%).

출처 및 근거

ORD 기록: ord-bd3cdf7f61004258875434e344fceaf3
출처 데이터셋: uspto-grants-2016_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09434718B2

반응 노트

불러오는 중…