Ammonia → HCID 178510951, 화합물

HRID 57283노트

반응식

HRID 57283 반응식
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[C:10]1[C:14]([CH2:15][CH2:16][CH2:17]Br)=[N:13][NH:12][C:11]=1[NH2:19].[NH2:20]C1NN=C(CCCO)C=1C1SC2C=CC=CC=2N=1.N>C(O)C>[NH2:20][CH2:17][CH2:16][CH2:15][C:14]1[C:10]([C:2]2[S:1][C:5]3[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=3[N:3]=2)=[C:11]([NH2:19])[NH:12][N:13]=1

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 178509116HCID 178509116, 화합물HCID 178509119HCID 178509119, 화합물

생성물 1

HCID 178510951HCID 178510951, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The title compound (12 mg) was prepared using 130 mg (0.39 mmol) of 4-benzothiazol-2-yl-5-(3-bromopropyl)-2H-pyrazol-3-ylamine, which was derived from 3-(5-amino-4-benzothiazol-2-yl-1H-pyrazol-3-yl)-propan-1-ol, and a saturated solution of ammonia gas in ethanol. MS (m/z, ES+): 274.2 (M+1, 100%), 257.2 (M−NH2, 70%).

출처 및 근거

ORD 기록
ord-30e4b5a6c43c493ca59a60ebd6f0daaa
출처 데이터셋
uspto-grants-2016_09
특허 번호
US09434720B2

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