Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → HCID 178503348, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | HCID 178527819 | HCID 178527819 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 178503348 | HCID 178503348 | 22% |
반응 단계
To a solution of 1H-imidazo[4,5-b]pyridine-2-thiol (5.0 g) in acetone (75 mL) were added MeI (2.3 mL) and K2CO3 (18 g) at room temperature. After stirring for 1 day, the mixture was filtered and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (AcOEt/hexane) to give the title compound (1.2 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09029536B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-83f8525bd2344d57981d3734115d833a |
| 출처 메모 | uspto-grants-2015_05 |