5-Bromo-2-chloro-3,4-dimethoxybenzoic acid → 5-Bromo-2-chloro-N,3,4-trimethoxy-N-methylbenzamide

HRID 576406노트

반응식

HRID 576406 반응식
[CH2:1]([O:4][C:5]1[C:6]([Cl:18])=[C:7]([CH:14]=[C:15]([Br:17])[CH:16]=1)[C:8]([N:10]([O:12][CH3:13])[CH3:11])=[O:9])C=C.BrC1C(OC)=C(OC)C(Cl)=C(C=1)[C:25](O)=[O:26]>>[Br:17][C:15]1[C:16]([O:26][CH3:25])=[C:5]([O:4][CH3:1])[C:6]([Cl:18])=[C:7]([CH:14]=1)[C:8]([N:10]([O:12][CH3:13])[CH3:11])=[O:9]

참가 물질

3

반응물 2

HCID 867140755-Bromo-2-chloro-3,4-dimethoxybenzoic acidHCID 892838625-bromo-2-chloro-N-methoxy-N-methyl-3-prop-2-enoxybenzamide

생성물 1

HCID 892531805-Bromo-2-chloro-N,3,4-trimethoxy-N-methylbenzamide

실험 절차

Similar procedure with preparation of 182 proceeded except for using compound 158 to obtain the compound 195.

출처 및 근거

ORD 기록
ord-5e201ffb70254f68960121727503ae6d
출처 데이터셋
uspto-grants-2015_05
특허 번호
US09034921B2

반응 노트

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