Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyldioxirane → 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyldioxirane | HCID 115197 | — |
| 반응물 | 8-Benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one | HCID 22499178 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one | HCID 57494231 | — |
반응 단계
To 8-benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one (300 mg) is added to a 0.1M solution of dimethyldioxirane in acetone (12.4 mL). After stirring at room temperature for 2 hours, the solvent is removed in vacuo to yield the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09040559B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-eb7320f580da452e86c706135ebd2912 |
| 출처 메모 | uspto-grants-2015_05 |