Water → Adipic acid di(2-propylidene hydrazide)

HRID 578613

반응식

HRID 578613 반응식
O.[C:2]([NH:12][NH2:13])(=[O:11])[CH2:3][CH2:4][CH2:5][CH2:6][C:7]([NH:9][NH2:10])=[O:8]>CC(=O)C>[CH:2](=[N:10][NH:9][C:7](=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][C:2]([NH:12][N:13]=[CH:5][CH2:6][CH3:7])=[O:11])[CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 962WaterHCID 66117Adipic Dihydrazide

생성물 1

HCID 86666342Adipic acid di(2-propylidene hydrazide)

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

In a stainless steel flask equipped with an agitator, 58.6 grams of water were added, the agitator was turned on, then 25 grams of adipic acid dihydrazide were added. The mixture was agitated for at least 10 minutes until a stable dispersion was formed. 16.4 grams of 2-propanone were then added under mixing. A clear solution formed after a few minutes. Mixing was continued for at least another hour until reaction product precipitated and formed a stable dispersion.

후처리

  1. additionwere added
  2. additionwere added
  3. customwas formed
  4. additionunder mixing
  5. customA clear solution formed after a few minutes
  6. additionMixing
  7. customuntil reaction product
  8. customprecipitated
  9. customformed a stable dispersion

출처 및 근거

ORD 기록
ord-59e99d01d81845d1a2b7979ebe0a412e
출처 데이터셋
uspto-grants-2015_05
특허 번호
US09040617B2

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