Water → Adipic acid di(2-propylidene hydrazide)

HRID 578614

반응식

HRID 578614 반응식
O.[C:2]([NH:12][NH2:13])(=[O:11])[CH2:3][CH2:4][CH2:5][CH2:6][C:7]([NH:9][NH2:10])=[O:8]>CC(=O)C>[CH:2](=[N:10][NH:9][C:7](=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][C:2]([NH:12][N:13]=[CH:5][CH2:6][CH3:7])=[O:11])[CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 962WaterHCID 66117Adipic Dihydrazide

생성물 1

HCID 86666342Adipic acid di(2-propylidene hydrazide)

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

In a stainless steel flask equipped with an agitator, 54.6 grams of water were added, the agitator was turned on, then 25 grams of adipic acid dihydrazide were added. The mixture was agitated for at least 10 minutes until a stable dispersion was formed. 16.4 grams of 2-propanone were then added under mixing. A clear solution formed after a few minutes. Mixing was continued for at least another hour until reaction product precipitated and formed a stable dispersion. 4 grams of AQUAFLOW NLS-200 (rheology additive) were added to the dispersion under agitation.

후처리

  1. additionwere added
  2. additionwere added
  3. customwas formed
  4. additionunder mixing
  5. customA clear solution formed after a few minutes
  6. additionMixing
  7. customuntil reaction product
  8. customprecipitated
  9. customformed a stable dispersion
  10. addition4 grams of AQUAFLOW NLS-200 (rheology additive) were added to the dispersion under agitation

출처 및 근거

ORD 기록
ord-a13547bbd5534e7babd37c566b65c98f
출처 데이터셋
uspto-grants-2015_05
특허 번호
US09040617B2

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