Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromodibenzofuran → 2,8-Dibromodibenzofuran
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromodibenzofuran | HCID 6856 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 생성물 | 2,8-Dibromodibenzofuran | HCID 82290 | 50% |
반응 단계
The procedure for the synthesis of 19 was followed (1 eq. bromine was used) to prepare 20 from 19 as white crystals in a 50% yield. 1H NMR (400 MHz, CDCl3, 298 K): δ(ppm) 8.04-8.03 (d, J=2.00 Hz, 2H), 7.60-7.59 (d, J=2.00 Hz, 1H), 7.58-7.57 (d, J=2.00 Hz, 1H), 7.47 (s, 1H), 7.44 (s, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09040718B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-74a311f78c3d4e65b469c52b1ba6431f |
| 출처 메모 | uspto-grants-2015_05 |