Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminobenzoic Acid → p-((1-Oxoallyl)amino)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminobenzoic Acid | HCID 978 | — |
| 반응물 | Acryloyl chloride | HCID 13140 | — |
| 반응물 | Aminobenzoic acid hydrochloride | HCID 12209225 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | p-((1-Oxoallyl)amino)benzoic acid | HCID 84866 | 78.8% |
반응 단계
0.66 g (7.3 mmoles) of acryloyl chloride was added to a solution of 2 g (14.3 mmoles) of p-aminobenzoic acid in 40 mL tetrahydrofuran (THF). A white precipitate consisting of p-aminobenzoic acid hydrochloride formed. The suspension was filtered and the filtrate was dried by vacuum evaporation to yield 1.1 g p-acrylamidobenzoic acid (reaction shown in FIG. 16a).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04749647 |
| 출처 데이터셋 | uspto-grants-1988_06 |
| ORD ID | ord-bee312e1396e42e4aee42cf412906e72 |
| 출처 메모 | uspto-grants-1988_06 |