Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroquinone → Triphenylmethyl acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroquinone | HCID 785 | — |
| 반응물 | Trityl chloride | HCID 6456 | — |
| 반응물 | Potassium acrylate | HCID 4429391 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Triphenylmethyl acrylate | HCID 12641354 | — |
반응 단계
1 mole triphenylchloromethane was stirred with 1.5 moles potassium acrylate in 998 g dimethyl formamide in the presence of 0.14 g hydroquinone under the conditions described in Example 1. The precipitated potassium chloride was filtered off and the triphenyl methyl acrylate solution was concentrated by rotary evaporation at 65° to 100° C. and reduced to produce liquid triphenylmethyl acrylate. This was dissolved at 70 percent in xylene and filtered.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04752629 |
| 출처 데이터셋 | uspto-grants-1988_06 |
| ORD ID | ord-7e5b6cf23b4a4a57b26e02bf28097737 |
| 출처 메모 | uspto-grants-1988_06 |