Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → 1,4-Bis(4-vinylbenzylamino) anthraquinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | 2,6-Lutidine | HCID 7937 | — |
| 반응물 | Solvent Blue 68 | HCID 20419 | — |
| 반응물 | p-Vinylbenzyl chloride | HCID 74126 | — |
| 생성물 | 1,4-Bis(4-vinylbenzylamino) anthraquinone | HCID 11123531 | — |
반응 단계
Reaction was performed by using the following reactants, catalyst and solvent: 1-amino-4-anilinoanthraquinone (precursor, 2.5 g, 7.96 mmol), 4-vinylbenzyl chloride (1.25 g, 8.22 mmol), 2,6-lutidine (a catalyst, 0.88 g, 8.22 mmol) and acetonitrile (solvent, 25 ml) in a reaction apparatus similar to that of Example 1. After completion of the reaction, the product was purified in the same manner as in Example 1 to afford the desired reactive dye, BD-4 (Yield: 67%). ##STR9##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05919880 |
| 출처 데이터셋 | uspto-grants-1999_07 |
| ORD ID | ord-c489318c97f3481899e8a8ad54ac2ea8 |
| 출처 메모 | uspto-grants-1999_07 |