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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 581185생성일: 2026년 10월 26일

Acetonitrile → 1,4-Bis(4-vinylbenzylamino) anthraquinone

https://huagongshe.com/reaction/581185

반응식

참여 물질

역할이름HCID투입량
반응물AcetonitrileHCID 6342—
반응물2,6-LutidineHCID 7937—
반응물Solvent Blue 68HCID 20419—
반응물p-Vinylbenzyl chlorideHCID 74126—
생성물1,4-Bis(4-vinylbenzylamino) anthraquinoneHCID 11123531—

반응 단계

Reaction was performed by using the following reactants, catalyst and solvent: 1-amino-4-anilinoanthraquinone (precursor, 2.5 g, 7.96 mmol), 4-vinylbenzyl chloride (1.25 g, 8.22 mmol), 2,6-lutidine (a catalyst, 0.88 g, 8.22 mmol) and acetonitrile (solvent, 25 ml) in a reaction apparatus similar to that of Example 1. After completion of the reaction, the product was purified in the same manner as in Example 1 to afford the desired reactive dye, BD-4 (Yield: 67%). ##STR9##

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05919880
출처 데이터셋uspto-grants-1999_07
ORD IDord-c489318c97f3481899e8a8ad54ac2ea8
출처 메모uspto-grants-1999_07