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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 581881생성일: 2026년 10월 26일

Pyridine → 2-(Cyclopent-3-en-1-yl)ethyl toluenesulfonate

https://huagongshe.com/reaction/581881

반응식

참여 물질

역할이름HCID투입량
반응물PyridineHCID 1049—
반응물4-Toluenesulfonyl chlorideHCID 7397—
반응물3-Cyclopentene-1-ethanolHCID 15749002—
생성물2-(Cyclopent-3-en-1-yl)ethyl toluenesulfonateHCID 8675422160.8%

반응 단계

A para-toluenesulfonylchloride (3.81 g, 20 mmol) was added to the pyridine (30 ml) solution of 2-(cyclopent-3-en-1-yl)ethyl alcohol (2.24 g, 20 mmol) and then the reaction mixture was stirred at room temperature for 2 hrs. After the removement of pyridine, the residue was extracted with dichloromethane, washed with 1N HCl, dried, filtered and separated by column chromatography to give a desirable product (3.24 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05922727
출처 데이터셋uspto-grants-1999_07
ORD IDord-33cf5353fbfa4e159987f8de76ce1c8d
출처 메모uspto-grants-1999_07