Sulfuric Acid → 1-(4-amino-3-nitrophenyl)ethanone
반응식
[C:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10]C(=O)C)=[C:6]([N+:14]([O-:16])=[O:15])[CH:5]=1)(=[O:3])[CH3:2].S(=O)(=O)(O)O>O>[C:1]([C:4]1[CH:9]=[CH:8][C:7]([NH2:10])=[C:6]([N+:14]([O-:16])=[O:15])[CH:5]=1)(=[O:3])[CH3:2]참가 물질
4
실험 절차
N-(4-acetyl-2-nitrophenyl)acetamide (26.5 g, 11.94 mmol) was added to a mixture of water and concentrated sulfuric acid, 150 ml (1:2). After 15 minutes the mixture was poured into water. The product was filtered off, washed with water and dried.
후처리
- filtrationThe product was filtered off
- washwashed with water
- customdried
출처 및 근거
- ORD 기록
- ord-4cd9d2f8740145f98a89fec295a82ac8
- 출처 데이터셋
- uspto-grants-1999_07
- 특허 번호
- US05922724
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