Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(3-Nitrophenyl)pyridine → 3-(Pyridin-3-yl)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(3-Nitrophenyl)pyridine | HCID 12181327 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(Pyridin-3-yl)aniline | HCID 459521 | — |
반응 단계
3-(3-pyridyl)-nitrobenzene (9.1 g, 45.5 mmol) in ethanol (125 ml) is hydrogenated at ambient pressure for 1.75 hours using Raney Nickel as the catalyst. Filtration of the resulting solution through celite followed by evaporation of solvent quantitatively yields 3-(3-pyridyl)aniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05922724 |
| 출처 데이터셋 | uspto-grants-1999_07 |
| ORD ID | ord-e2c51de4f901493c8a5c8e21efe583c1 |
| 출처 메모 | uspto-grants-1999_07 |