참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | SR142948A | HCID 5311451 | — |
| 반응물 | HCID 178418600 | HCID 178418600 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178491337 | HCID 178491337 | 43.9% |
반응 단계
0.1 g of the compound obtained in EXAMPLE 1' and 0.03 g of (S)-(+)-arginine are dissolved in the heated state in 4 ml of MeOH, and this solution is concentrated to 1 ml and poured into 10 ml of ether cooled to 5° C. 0.055 g of the expected product is obtained after draining and drying over P2O5, m.p.=176° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05925661 |
|---|
| 출처 데이터셋 | uspto-grants-1999_07 |
|---|
| ORD ID | ord-f0c9d091fd4c4411a273b17466d68ea3 |
|---|
| 출처 메모 | uspto-grants-1999_07 |
|---|
