Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 5,6-Dichloronicotinate → Dimethyl 3-Chloro-2,6-pyridinedicarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 5,6-Dichloronicotinate | HCID 2782166 | — |
| 반응물 | 2,3-Dichloro-5-(methoxymethyl)pyridine | HCID 11137960 | — |
| 생성물 | Dimethyl 3-Chloro-2,6-pyridinedicarboxylate | HCID 53845654 | 73% |
반응 단계
Example 2 was repeated, except that the 2,3-dichloro-5-(methoxymethyl)pyridine was replaced by the same molar amount of methyl 2,3-dichloro-5-pyridinecarboxylate. After a reaction time of 6 hours at a bath temperature of 160° C., 1.20 g (73 percent) of a yellow product was obtained. Other data concerning the product was:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05925765 |
| 출처 데이터셋 | uspto-grants-1999_07 |
| ORD ID | ord-09075152a86f4f358289b2225de3bb1c |
| 출처 메모 | uspto-grants-1999_07 |