Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → 3-Bromo-2-methoxy-5-nitropyridine

HRID 583173

반응식

HRID 583173 반응식
[OH:1][C:2]1[C:7]([Br:8])=[CH:6][C:5]([N+:9]([O-:11])=[O:10])=[CH:4][N:3]=1.F[B-](F)(F)F.[CH3:17][O+](C)C>C(Cl)Cl>[CH3:17][O:1][C:2]1[C:7]([Br:8])=[CH:6][C:5]([N+:9]([O-:11])=[O:10])=[CH:4][N:3]=1

참가 물질

4

반응물 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 178526832HCID 178526832, 화합물

생성물 1

HCID 215844513-Bromo-2-methoxy-5-nitropyridine

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The title compound was synthesized from 2-hydroxy-3-bromo-5-nitropyridine by the method of H. J. W. van den Haak et al, Recl.Trav. Chim. Pays-Bas 99(3), p83-87 (1980) using trimethyloxonium tetrafluoroborate in methylene chloride.

출처 및 근거

ORD 기록
ord-9cb449e7728f42ea8e324a1151c950ec
출처 데이터셋
uspto-grants-1999_07
특허 번호
US05929094

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