Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
12-Methoxydodecanoate → 12-Methoxydodecanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 12-Methoxydodecanoate | HCID 1420 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 12-Methoxy-N-(phenylmethyl)dodecanamide | HCID 9797119 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 12-Methoxydodecanoyl chloride | HCID 19611759 | — |
반응 단계
Reaction Scheme 4 illustratively shows the preparation of 12-methoxy-N-(phenyl-methyl)dodecanamide wherein 12-methoxydodecanoic acid (8) is treated with oxalyl chloride in anhydrous toluene to form 12-methoxydodecanoyl chloride (9) which in turn reacts with benzylamine in methylene chloride to give the desired fatty acid amide (10).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05929110 |
| 출처 데이터셋 | uspto-grants-1999_07 |
| ORD ID | ord-18409ab56e9146fa80ab1f57f2103424 |
| 출처 메모 | uspto-grants-1999_07 |