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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 583666생성일: 2026년 10월 27일

Hydrochloric Acid → 4-(2-Aminoethyloxy)benzoyl-2(S)-phenylsulfonylamino-beta-alanine-HCl

https://huagongshe.com/reaction/583666

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물1,4-DioxaneHCID 31275—
반응물4-[2-(N-BOC-Amino)ethyloxy]benzoyl-2(S)-phenylsulfonylamino-beta-alanine tert-butyl esterHCID 10840664—
생성물4-(2-Aminoethyloxy)benzoyl-2(S)-phenylsulfonylamino-beta-alanine-HClHCID 86754335—

반응 단계

A suspension of 2-3 (105 mg, 0.19 mmol) in 6N HCl (5 mL) was treated with dioxane (5 mL) to effect a homogeneous solution. After stirring for 20 h at ambient temperature, the solvents were evaporated and the resulting residue azeotroped with toluene to afford 12-1 as a colorless solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05929120
출처 데이터셋uspto-grants-1999_07
ORD IDord-3545c1a839b84107a6729d4bc39d022f
출처 메모uspto-grants-1999_07