Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3-Bromo-4-methylphenyl)methanol → 3-Bromo-4-methylbenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3-Bromo-4-methylphenyl)methanol | HCID 12947381 | — |
| 촉매 | Manganese oxide | HCID 160959 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-Bromo-4-methylbenzaldehyde | HCID 816765 | 85% |
반응 단계
14.4 g (72 mmol) of (3-bromo-4-methylphenyl)methanol are placed in 200 ml of dichloromethane in a round-bottomed flask. 62.6 g (72 mmol) of manganese oxide are added and the medium is stirred at room temperature overnight. The mixture is filtered through Celite and the solvent is evaporated off. 11.8 g (85%) of the expected product are obtained in the form of an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06924400B2 |
| 출처 데이터셋 | uspto-grants-2005_08 |
| ORD ID | ord-20172710c0904141ac8730fb33bb8ee2 |
| 출처 메모 | uspto-grants-2005_08 |