4-Formylphenylboronic Acid → HCID 86591268, 화합물

HRID 584905

반응식

HRID 584905 반응식
Br[C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[CH2:5][N:6]([CH3:14])[C:7](=[O:13])[O:8][C:9]([CH3:12])([CH3:11])[CH3:10].[CH:18]([C:20]1[CH:25]=[CH:24][C:23](B(O)O)=[CH:22][CH:21]=1)=[O:19]>>[CH:18]([C:20]1[CH:25]=[CH:24][C:23]([C:2]2[CH:17]=[CH:16][CH:15]=[C:4]([CH2:5][N:6]([CH3:14])[C:7](=[O:13])[O:8][C:9]([CH3:12])([CH3:11])[CH3:10])[CH:3]=2)=[CH:22][CH:21]=1)=[O:19]

참가 물질

3

반응물 2

HCID 5910734-Formylphenylboronic AcidHCID 20738487tert-Butyl 3-bromobenzyl(methyl)carbamate

생성물 1

HCID 86591268HCID 86591268, 화합물

실험 절차

In a manner similar to that of Example 1(e) by reacting 13.7 g (45 mmol) of tert-butyl (3-bromo benzyl)-N-methylcarbamate (prepared in Example 1(b)) with 10 g (67 mmol) of 4-formylbenzene-boronic acid, 11 g (76%) of the expected are obtained.

후처리

  1. customexpected are obtained

출처 및 근거

ORD 기록
ord-c5d4ef180d83456ba7a1d9506c292c2d
출처 데이터셋
uspto-grants-2005_08
특허 번호
US06927228B2

연결된 노트

불러오는 중…