Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 1-Nitro-2,5-bis(trifluoromethyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 1,4-Bis(trifluoromethyl)benzene | HCID 67945 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | 1-Nitro-2,5-bis(trifluoromethyl)benzene | HCID 2734048 | 35% |
반응 단계
A process of nitrating 1,4-bis(trifluoromethyl)benzene by means of 100 mass % nitric acid at from 90 to 105° C. by using 24% fuming sulfuric acid as a solvent to obtain 2,5-bis(trifluoromethyl)nitrobenzene in a yield of 35% (J. Amer. Chem. Soc., 75, 4967 (1953)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06930214B2 |
| 출처 데이터셋 | uspto-grants-2005_08 |
| ORD ID | ord-a644530108b94ad983475f442eb57f48 |
| 출처 메모 | uspto-grants-2005_08 |