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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 585393생성일: 2026년 10월 26일

1-Hexanethiol → 9-[1-(3,4-Dimethoxybenzoyl)-2-[5-(hexylthio)pentyl]-1,2,3,4-tetrahydro-4-quinolinyl]-9H-carbazole

https://huagongshe.com/reaction/585393

반응식

참여 물질

역할이름HCID투입량
반응물1-HexanethiolHCID 8106—
반응물5-[4-(9H-9-Carbazolyl)-1-(3,4-dimethoxybenzoyl)-1,2,3,4-tetrahydro-2-quinolinyl]-1-pentanolHCID 22339233—
생성물9-[1-(3,4-Dimethoxybenzoyl)-2-[5-(hexylthio)pentyl]-1,2,3,4-tetrahydro-4-quinolinyl]-9H-carbazoleHCID 223392747%

반응 단계

Starting with 5-[4-(9H-9-carbazolyl)-1-(3,4-dimethoxybenzoyl)-1,2,3,4-tetrahydro-2-quinolinyl]-1-pentanol (0.08 g, 0.15 mmol) prepared in Example 135 and n-hexylmercaptan (0.3 ml), the same procedure as shown in Example 136 was repeated to give the titled compound (0.01 g, yield: 7%) as a white crystal (cis:trans=6:1).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06930104B2
출처 데이터셋uspto-grants-2005_08
ORD IDord-22b2ffa25a3a4a679202a7619554e586
출처 메모uspto-grants-2005_08