Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 5-(3-Bromophenyl)-1H-1,2,4-triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 5-(3-Bromophenyl)-1-(2-trimethylsilanylethoxymethyl)-1H-[1,2,4]triazole | HCID 22329519 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-(3-Bromophenyl)-1H-1,2,4-triazole | HCID 12461546 | 89.3% |
반응 단계
This reaction was carried out as described in Example 40, step b, using 5-(3-bromophenyl)-1-(2-trimethylsilanylethoxymethyl)-1H-[1,2,4]triazole (2.88 g, 8.1 mmol), 2 N HCl (50 ml) and ethanol (50 ml) to yield the title compound (1.62 g, 89%): 1H NMR (360 MHz, DMSO-d6) δ 8.70 (1H, s), 8.16 (1H, s), 8.01 (1H, d, J 7.8 Hz), 7.63 (1H, d, J 7.8 Hz), 7.46 (1H, t, J 7.8 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06936608B2 |
| 출처 데이터셋 | uspto-grants-2005_08 |
| ORD ID | ord-ed683daacb8b4ec984001d9b2ef31b96 |
| 출처 메모 | uspto-grants-2005_08 |