HCID 86595801, 화합물 → HCID 86759824, 화합물

HRID 586661노트

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HRID 586661 반응식
[CH3:1][O:2][CH2:3][C@@H:4]1[C@H:6]([CH:7]=[O:8])[C@:5]1([CH3:23])[C:9]1[CH:18]=[CH:17][C:16]2[C:15]([CH3:20])([CH3:19])[CH2:14][CH2:13][C:12]([CH3:22])([CH3:21])[C:11]=2[CH:10]=1.CC12C(C)(C)C(C(OC[C@@H]3[C@@H](COC)[C@]3(C)C3C=CC4C(C)(C)CCC(C)(C)C=4C=3)=O)(CC1)OC2=O>>[CH3:1][O:2][CH2:3][C@@H:4]1[C@@H:6]([CH:7]=[O:8])[C@@:5]1([CH3:23])[C:9]1[CH:18]=[CH:17][C:16]2[C:15]([CH3:20])([CH3:19])[CH2:14][CH2:13][C:12]([CH3:22])([CH3:21])[C:11]=2[CH:10]=1

참가 물질

3

반응물 2

HCID 86595801HCID 86595801, 화합물HCID 86759822HCID 86759822, 화합물

생성물 1

HCID 86759824HCID 86759824, 화합물수율 81%

실험 절차

Following a procedure similar to that for the preparation of Intermediate 12a but using Intermediate 11a as the starting material afforded the title compound (25 mg, 81% yield) as a colorless oil:

출처 및 근거

ORD 기록
ord-1431d0afe25b4f2ab654bce515913b64
출처 데이터셋
uspto-grants-2005_08
특허 번호
US06936636B2

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