Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromopropane → Methyl 4-(5-bromo-2-cyano-1-methoxy-1-oxopentan-2-yl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromopropane | HCID 6358 | — |
| 반응물 | Dimethyl Carbonate | HCID 12021 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| 반응물 | Methyl 4-(cyanomethyl)benzoate | HCID 848548 | — |
| 반응물 | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| 생성물 | Methyl 4-(5-bromo-2-cyano-1-methoxy-1-oxopentan-2-yl)benzoate | HCID 59419916 | — |
반응 단계
For Step 1, methyl 4-(cyanomethyl)benzoate was substituted for (3,4-Dimethoxyphenyl)acetonitrile and dimethyl carbonate was substituted for 2-bromopropane. For Step 2, sodium hydride was substituted for NaHMDS.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09227918B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-93172768202b488bbf9cd50f45bba093 |
| 출처 메모 | uspto-grants-2016_01 |